By Qisheng Lin, John D. Corbett (auth.), Prof. Dr. Xin-Tao Wu (eds.)
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Additional info for Controlled Assembly and Modification of Inorganic Systems
Generally, the preparation conditions of peripherally functionalized Pcs based on substituted precursors are softer than those employed in the synthesis of conventional unsubstituted Pcs, because the increased solubility of starting substituted precursors and the resulting peripherally substituted Pcs allow the employment of a wide variety of solvents. The peripherally substituted ligands mainly include crown ether, alkyl, alkoxy and alkylthio groups. From the point of view of symmetry, this type of Pc includes symmetrically and unsymmetrically substituted Pcs.
In addition, further examination of the bands for the 1/1 AC reveal that the pseudogap arises largely from mixing between s, p orbitals of Cu and Ga with the low-lying d of Sc and that these also enhance the depth of the pseudogap. All of these parallel earlier theoretical results for (Ca,Yb)Cd6 reported by Ishii and Fujiwara . 5 311001 222000 320000 320020 222110 311200 221210 211112 311111 222111 311000 211101 221001 301001 111111 211000 211010 111100 111110 210010 111000 Q. D. 0 20 25 30 35 40 45 50 55 60 65 70 2q (º) Fig.
In 2002, Janczak and co-workers  characterized the crystal structure of CrIII Pc(I)2 · I2 (3). The central CrIII ion is coordinated by four Niso atoms from the one-electron oxidized Pc(1-) macrocyclic radical ligand and two trans iodine atoms, yielding a distorted CrN4 I2 octahedral geometry. CrIII (Pc)(I)2 units are connected together by type C Pc π–π interactions, forming slipped-stacked 1D columnar struc˚ The tures as shown in Fig. 7. 402 A. 6◦ , which is markedly smaller than those of β-form parent MPcs without axial ligands (ca.