By B. R. Banerjee, W. D. Bingle (auth.), J. E. Forrette, E. Lanterman (eds.)
Read or Download Developments in Applied Spectroscopy: Proceedings of the Fourteenth Annual Mid-America Spectroscopy Symposium Held in Chicago, Illinois, May 20–23, 1963 PDF
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Additional resources for Developments in Applied Spectroscopy: Proceedings of the Fourteenth Annual Mid-America Spectroscopy Symposium Held in Chicago, Illinois, May 20–23, 1963
Three types of applieation are illustrated. The multichannel analyzer replaees a seanning crystal spectrometer for quick identifieation and semiquantitative analysis of components. Quantitative analysis by mathematical unfolding of the energy spectra is made praetical by the fast data collection of standard and unknown speetra; eomparison of results by unfolding and from crystal spectrometer data shows differences of less than 4% of the amount present. Quantitative two-dimensional topographie display is obtained by multisealer operation of the 400-channel memory system.
Fig. 6. Topographie display of precipitates in 7075 alloy in terms of Fe Ka radiation: (a) using automatie beam sweep in eleetron probe; (h) quantitative topographie display of same area using multiehannel analyzer in multisealer mode of operation. low total concentration of iron, it is difficult to reach any quantitative conclusions about the variations. The multichanne1 analyzer allows the display to be placed on a more quantitative basis by use of the multiscaler mode of operation described in the section on Equipment and Operation.
Next, the spectra from two unknown precipitates (Fig. 4b) were recorded and the total intensities were determined at the Fe, Cu, and Zn positions as shown in Table IlI. The desired L. S. BIRKS AND A. P. 4-min time. values to be found are the relative X-ray intensities, R Fe , R cu ' and R zn , for the three elements in the precipitates. 6%. 0%. As a check on the unfolding technique, crystal spectrometer data for the three standards and the precipitates were obtained simultaneously with the multichannel analyzer data.