Inorganic Synthesis, Vol. 31 by Alan H. Cowley

By Alan H. Cowley

The volumes during this carrying on with sequence offer a compilation of present ideas and ideas in inorganic man made chemistry. contains inorganic polymer syntheses and preperation of significant inorganic solidsd, sutheses utilized in the advance of pharamacologically lively inorganic compounds, small-molecule coordination complexes, and similar compounds. additionally comprises calcuable details on transition organometallic compunds, together with species with meta-metal cluster molecules. All syntheses provided right here were proven.

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Chem. , 1735 (1991). 14. M. Bochmann, A. P. Coleman, K. J. Webb, M. B. Hursthouse, and M. Mazid, Angew. , 103,973 (1991); Angew. Chem. Int. Ed. , 30,973 (1991);M. Bochmann, G. C. Bwembya, A. K. Powell, and X . Song, Polyhedron 14, 3495 (1995). 6. ARENE THIOLATO, SELENOLATO, AND TELLUROLATO COMPLEXES OF MERCURY SUBMITTED BY MANFRED BOCHMANN*' and KEVIN J. WEBB* CHECKED BY M. A. MALIK and P. O'BRIEN' Chalcogenolato complexes of mercury can be prepared by a variety of methods. Early preparations involve the reactions of thiols with mercury cyanide,' the reaction of mercury salts with alkali chalcogenolates, electrochemical methods,' and the oxidative addition of dichalcogenides to metallic m e r c ~ r y The .

103,973 (1991); Angew. Chem. Int. Ed. , 30,973 (1991);M. Bochmann, G. C. Bwembya, A. K. Powell, and X . Song, Polyhedron 14, 3495 (1995). 6. ARENE THIOLATO, SELENOLATO, AND TELLUROLATO COMPLEXES OF MERCURY SUBMITTED BY MANFRED BOCHMANN*' and KEVIN J. WEBB* CHECKED BY M. A. MALIK and P. O'BRIEN' Chalcogenolato complexes of mercury can be prepared by a variety of methods. Early preparations involve the reactions of thiols with mercury cyanide,' the reaction of mercury salts with alkali chalcogenolates, electrochemical methods,' and the oxidative addition of dichalcogenides to metallic m e r c ~ r y The .

J. A. Davies and S. G. Dutremez, J . Am. Ceram. ,73,2570 (1990). Inorganic Syntheses, Volume31 Edited by Alan H . Cowley Copyright © 1997 by Inorganic Syntheses, Inc. 4 . N-donor adducts of dimethylzinc 15 4. N-DONOR ADDUCTS OF DIMETHYLZINC SUBMITTED BY ANTHONY C. JONES,* PAUL O'BRIEN,' and JOHN R. WALSH' CHECKED BY BRIDGETT KILLION,' JOHN CANBELL,' STEPHEN SKOOG,' and WAYNE GLADFELTER' Although adducts between dimethylzinc(MezZn)and nitrogen donor ligands have been known for many years,'. they have only recently found a technological application as precursors in the growth of zinc chalcogenides by MOCVD,3-5 and as the dopant sources in the growth of 111-V materials6 by MOCVD.

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