Inorganic Chemistry of the Main-Group Elements Volume 3 A by C C Addison

By C C Addison

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Additional info for Inorganic Chemistry of the Main-Group Elements Volume 3 A review of the literature published between September 1973 and September 1974

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In principle, synthesis of the complexes is simple. g. ethanol, and warmed. Crystals separate on cooling. r. frequency of the polyether. The known compositions of LiX, NaX, and KX complexes with the four macrocyclic ethers are collected in Table 4. Two lithium compounds with (1) are established as monohydrated 1:1 complexes, the bromide and iodide. lo7 A generalized picture of the sodium and potassium complexes is shown in Figure 2. Complexes have also been prepared where X is an organic anion obtained by the deprotonation of 2-nitrophenol, 4-nitrophenol, 2,4-dinitrophenol, 2,4,6-trinitrophenol, 2-hydroxybenzoic acid, 2,6-dihydroxybenzoic acid, 2nitrobenzoic acid, or 2-aminobenzoic acid.

Strukt. , 1974,15,261. N. V. Novozhilova, T. N. Polynova, M. A. Porai-Koshits, N. I. Pechurova, L. I. Martynenko, and Ali Khadi, Zhur. strukt. , 1973, 14, 745. S. H. Shitlow, Inorg. , 1973, 12, 2286. 32 Inorganic Chemistry of the Main -group Elements Figure 13 A perspective view of the packing in NaCu(nta),H,O. The view, looking down the b-axis, selectively shows the basic nta structure, the metal atoms to which it bonds, and complete Cu and Na co -ordinations. (Reproduced by permission from Inorg.

18 kcal mol-'. p. 16' lS7 lS8 159 160 16' 162 Dz. Pelca, V. Brunere, and J. Sauka, Latu. R. Zinat. Akad. Vestis, Kim. , 1973, 390. R. C. , and L. Andrews, J. Chem. , 1973, 59, 1851. D. M. Lindsay, D . R. Herschback, and A . L. Kwiram, J. Chem. , 1974, 60, 315. V. Ya. Dadarev, A. B. Tsentsiper, and M. S. Dobrolyubova, Kristallografiya, 1973, 18, 759. S. P. Berardinelli and D . L. Draus, Inorg. , 1974, 13, 189. H. E. Flotow and D. W. Osborne, J. Chem. Thermodynamics, 1974, 6, 135. 28 kcal mol-'. '~" Interaction potentials of many ion pairs have been calculated assuming that the electron density of the combined system is equal to the sum of the two separate ionic electron densities.

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